تفاعل #994
ord-d2aea31453084c8dba037f866c0833b5
معادلة التفاعل
2-Methoxy-cinnamylalcohol
thionylchloride
piperazine
→
salt
N,N'-bis-((E)-3-(2-methoxyphenyl)-2-propenyl)piperazine
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىas described in Preparation Example 2
الإجراء التجريبي
2-Methoxy-cinnamylalcohol (1.44 g) was chlorinated using thionylchloride. Subsequently, reaction with piperazine and other treatments were performed as described in Preparation Example 2, to thereby obtain 314 mg of a salt as colorless prisms.