تفاعل #992696

ord-4f35ba68c5da457ab8339458b719f25e

معادلة التفاعل

O=C/C(Br)=C(/Br)C(=O)O
Mucobromic acid
N=C(N)NN.O=C(O)O
Aminoguanidine bicarbonate
O=C=O
carbon dioxide
NNC(N)=[NH2+].O=C/C(Br)=C(/Br)C(=O)[O-]
Aminoguanidinium Mucobromate

الكواشف

لا شيء

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThe water was removed in vacuo
  2. 2
    درجة الحرارةwith heating to approximately 90° C
  3. 3
    أخرىThe product was isolated as an off-white solid

الإجراء التجريبي

Mucobromic acid (2.0 g, 7.76 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (1.06 g, 7.76 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 18 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as an off-white solid.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08012277B2uspto-grants-2011_09