تفاعل #992696
ord-4f35ba68c5da457ab8339458b719f25e
معادلة التفاعل
Mucobromic acid
Aminoguanidine bicarbonate
carbon dioxide
→
Aminoguanidinium Mucobromate
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe water was removed in vacuo
- 2درجة الحرارةwith heating to approximately 90° C
- 3أخرىThe product was isolated as an off-white solid
الإجراء التجريبي
Mucobromic acid (2.0 g, 7.76 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (1.06 g, 7.76 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 18 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as an off-white solid.