تفاعل #992695

معادلة التفاعل

Nitrilotriacetic acid

Aminoguanidine bicarbonate

carbon dioxide

→

Tris(aminoguanidinium) Nitrilotriacetate

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   أخرىThe water was removed in vacuo
2. 2
   درجة الحرارةwith heating to approximately 90° C
3. 3
   أخرىThe product was isolated as a white solid

الإجراء التجريبي

Nitrilotriacetic acid (1.0 g, 5.23 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (2.14 g, 15.69 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for three days. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

المصدر