تفاعل #992694

معادلة التفاعل

Glycolic acid

Guanidine carbonate

carbon dioxide

→

Guanidinium Glycolate

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   أخرىThe water was removed in vacuo
2. 2
   درجة الحرارةwith heating to approximately 90° C
3. 3
   أخرىThe product was isolated as a white solid

الإجراء التجريبي

Glycolic acid (3.0 g, 39.45 mmol) was dissolved in 15 ml of distilled water. Guanidine carbonate (3.55 g, 19.72 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 4 hours. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

المصدر