تفاعل #992688

معادلة التفاعل

Oxalic acid

Guanidine carbonate

carbon dioxide

→

Bis(guanidinium) Oxalate

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   أخرىThe water was removed in vacuo
2. 2
   درجة الحرارةwith heating to approximately 90° C. for 4 hours
3. 3
   أخرىThe product was isolated as a white solid

الإجراء التجريبي

Oxalic acid (2.0 g, 22.20 mmol) was dissolved in 40 ml of distilled water. Guanidine carbonate (4.0 g, 22.20 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for one hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

المصدر