تفاعل #992687

معادلة التفاعل

Tetrafluorosuccinic acid

Guanidine carbonate

carbon dioxide

→

Bis(guanidinium) Tetrafluorosuccinate

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   أخرىThe water was removed in vacuo
2. 2
   درجة الحرارةwith heating to approximately 90° C. for 4 hours
3. 3
   أخرىThe product was isolated as a white solid

الإجراء التجريبي

Tetrafluorosuccinic acid (500 mg, 2.63 mmol) was dissolved in 10 ml of distilled water. Guanidine carbonate (474 mg, 2.63 mmol) was added at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 2 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

المصدر