تفاعل #992679

معادلة التفاعل

Hydrazine monohydrate

Trifluoroacetic acid

→

Hydrazinium TFA

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   workup.STIRRINGthe reaction was stirred at room temperature overnight
2. 2
   أخرىThe water was removed in vacuo
3. 3
   درجة الحرارةwith heating to 80° C.
4. 4
   أخرىyielding product as a colorless liquid

الإجراء التجريبي

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

المصدر