تفاعل #986705

ord-4cc4df8334944382abcfb07e83037bc4

معادلة التفاعل

O=[N+]([O-])c1ccc(-c2ccc(O)cc2)cc1
4-hydroxy-4′-nitrobiphenyl
COC(=O)c1ccc(CCl)o1
5-chloromethylfuran-2-carboxylic acid methyl ester
O=C(O)c1ccc(COc2ccc(-c3ccc([N+](=O)[O-])cc3)cc2)o1
5-(4′-Nitro-biphenyl-4-yloxymethyl)-furan-2-carboxylic acid

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

5-(4′-Nitro-biphenyl-4-yloxymethyl)-furan-2-carboxylic acid was prepared using general procedure A from 4-hydroxy-4′-nitrobiphenyl (available from TCI America, Portland, Oreg.) and 5-chloromethylfuran-2-carboxylic acid methyl ester (available from Aldrich, Milwaukee, Wis., or from Maybridge plc, Tintagel, UK). Yield: 40 mg. Mass spectrum (ES) MH+=340.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07355049B2uspto-grants-2008_04