تفاعل #985517

معادلة التفاعل

6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine

2-chloropyrimidine

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N-Pyrimidin-2-yl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

ظروف التفاعل

الإجراء التجريبي

N-Pyrimidin-2-yl-2,3,4,9-tetrahydro-1H-carbazol-1-amine was prepared from 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine (150 mg, 0.81 mmol) and 2-chloropyrimidine (184 mg, 1.62 mmol) in a similar manner as described in Example 22 to give 16 mg (8%) of a yellow solid. 1H-NMR (DMSO-d6): δ 10.63 (s, 1H), 8.32 (d, 2H), 7.43 (d, 1H), 7.36 (d, 1H), 7.25 (d, 1H), 7.01-6.97 (m, 1H), 6.93-6.89 (m, 1H), 6.60 (t, 1H), 5.32-5.28 (m, 1H), 2.68-2.57 (m, 2H), 2.041.97 (m, 2H), 1.87-1.75 (m, 2H).

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