تفاعل #985435

ord-ce1ebdbc7db04bf28aa7a39c4a3aba32

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

N-(5-Fluoro-2-nitrophenyl)-L-alanine was treated according to the procedure for the preparation of (3R)-3-ethyl-7-fluoro-3,4-dihydroquinoxalin-2(1H)-one (see Example 1) to yield (3S)-6-fluoro-3-methyl-3,4-dihydroquinoxalin-2(1H)-one. MS (ESI) m/z 181 ([M+H]+); Anal. Calcd for C9H9FN2O: C, 59.99; H, 5.03; N, 15.55. Found: C, 59.89; H, 4.88; N, 15.46.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07351709B2uspto-grants-2008_04