تفاعل #985434

ord-c68e23e8b24641ff8f46a33a79a15c92

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

2,4-Difluoronitrobenzene was treated with L-alanine according to the procedure for the preparation of (R)-2-(4-fluoro-2-nitrophenylamino)-butyric acid (see Example 1) to yield N-(5-fluoro-2-nitrophenyl)-L-alanine. MS (ESI) m/z 229 ([M+H]+); MS (ESI) m/z 227 ([M−H]−); Anal. Calcd for C9H9FN2O4: C, 47.37; H, 3.98; N, 12.28. Found: C, 47.61; H, 4.23; N, 12.39.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07351709B2uspto-grants-2008_04