تفاعل #971162

معادلة التفاعل

2-Amino-6-methyl-pyridine-3,5-dicarbonitrile

N,N-Dimethylformamide dimethyl acetal

→

title compound

المردود 94.0%

N′-(3,5-Dicyano-6-methyl-pyridin-2-yl)-N,N-dimethyl-formamidine

المردود 94.0%

المذيبات

toluene

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةat reflux for 6 hours
2. 2
   تركيزthe solution was concentrated under vacuum

الإجراء التجريبي

A solution of 2-Amino-6-methyl-pyridine-3,5-dicarbonitrile (0.158 g, 1.0 mmol) and N,N-Dimethylformamide dimethyl acetal (0.119 g, 1.0 mmol) in toluene (10 mL) was heated at reflux for 6 hours. After cooling to room temperature, the solution was concentrated under vacuum to provide the title compound as a brown solid (0.2 g, 94%).

المصدر