تفاعل #955933

معادلة التفاعل

methyl 2,4-dimethylbenzoate

hydrazine

→

2,4-dimethylbenzohydrazide

المذيبات

MeOH

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةthe mixture was heated
2. 2
   درجة الحرارةunder reflux for 40 hours
3. 3
   أخرىThen the mixture was evaporated
4. 4
   أخرىdried under vacuum

الإجراء التجريبي

To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).

المصدر