تفاعل #955921
ord-a615ba1b682243c6b46e338c458eba06
معادلة التفاعل
Methyl 4-ethyl-2-methylbenzoate
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title product
4-Ethyl-2-methylbenzoic acid
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
درجة الحرارة
60°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1غسيلThe mixture was washed with hexanes
الإجراء التجريبي
Methyl 4-ethyl-2-methylbenzoate (example 10c) (2.37 g) was dissolved in aq. NaOH (1M, 40 mL) and the solution heated at 60° C. overnight. The mixture was washed with hexanes and the aqueous layer was acidified with 6N HCl to pH 2. The title product was obtained as a white precipitate, following filtration and drying (2.17 g, 80%).