تفاعل #95323

معادلة التفاعل

product

2-isopropyl-2-p-chlorophenyl-acetic acid

thionyl chloride

→

2-isopropyl-2-p-chlorophenyl acetyl chloride

المذيبات

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةthe mixture was refluxed for 4 hours
2. 2
   درجة الحرارةwas then cooled
3. 3
   أخرىThe mixture was evaporated to dryness

الإجراء التجريبي

10 g of the product of Step D were added to a mixture of 50 ml of petroleum ether (b.p.=35°-70° C.) and 20 ml of thionyl chloride and the mixture was refluxed for 4 hours and was then cooled. The mixture was evaporated to dryness to obtain 10.8 g of D 2-isopropyl-2-p-chlorophenyl acetyl chloride.

المصدر