تفاعل #95279
ord-fe977b0fce07433485951a2064330411
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىgave 58 g
- 2أخرىThe oil is purified by adsorption chromatography on a magnesia silica gel column
- 3أخرىto give a light yellow oil
الإجراء التجريبي
Treatment of 63 g. (0.25 mole) of 1-iodo-trans-1-octen-3-one (Example 724) with sodium borohydride in the manner described in Example 726 gave 58 g. of yellow oil. The oil is purified by adsorption chromatography on a magnesia silica gel column using benzene as eluent to give a light yellow oil.