تفاعل #95091

ord-d96bdb1a6b4e4da1912ceaee73b6dc48

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The N-(1-methyldecyl)-3-(3-nitrophenyl)-2-butenamide from Preparation 23 (6.5 g.) was reduced with iron powder (5.0 g.) in glacial acetic acid (80 ml.) in a manner analogously to Preparation 27. After chromatography, 4.5 g. of the title compound was obtained, as an amber oil.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04343813uspto-grants-1982_08