تفاعل #95089

معادلة التفاعل

3-(3-nitrophenyl)-2-butenoic acid

ethyl chloroformate

1-methyldecylamine

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title product

المردود 72.0%

N-(1-Methyldecyl)-3-(3-Nitrophenyl)-2-butenamide

المردود 72.0%

ظروف التفاعل

المعالجة

1. 1
   أخرىaccording to the procedure of Preparation 22

الإجراء التجريبي

The 3-(3-nitrophenyl)-2-butenoic acid from Preparation 12 having a melting point of 147°-149° C. was reacted with ethyl chloroformate, followed by 1-methyldecylamine, according to the procedure of Preparation 22. This afforded a 72% yield of the title product.

المصدر