تفاعل #94256

معادلة التفاعل

3,7-dimethyl-7(t-butylperoxy)octyl alcohol

pyridine

n-butyl chloroformate

→

3,7-Dimethyl-7-(t-butylperoxy)octyl n-butyl carbonate

المذيبات

diethyl ether

diethyl ether

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةThe reaction temperature was maintained at 15°±1° C during the addition

الإجراء التجريبي

To a solution of 7.9 g (0.03 mole) of 3,7-dimethyl-7(t-butylperoxy)octyl alcohol and 2.4 g (0.03 mole) of pyridine in diethyl ether cooled at 10°±1° C was added a solution of 4.09 (0.03 mole) of n-butyl chloroformate in diethyl ether. The reaction temperature was maintained at 15°±1° C during the addition.

المصدر