تفاعل #94102

معادلة التفاعل

dimethyl adipate

sodium hydroxide

→

disodium adipate

المذيبات

acetonitrile

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةat reflux temperature for 18 hours
2. 2
   ترشيحThe resulting solution was filtered hot
3. 3
   أخرىdried

الإجراء التجريبي

17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.

المصدر