تفاعل #939043

معادلة التفاعل

2-Nitroresorcinol

→

desired compound

المردود 97.0%

2-Aminoresorcinol

المردود 97.0%

المذيبات

ethanol

ظروف التفاعل

المعالجة

1. 1
   أخرىInsolubles were removed by filtration
2. 2
   workup.DISTILLATIONthe solvent was distilled off under reduced pressure

الإجراء التجريبي

2-Nitroresorcinol (1.00 g, 6.45 mmol) was dissolved in ethanol (10 mL). The solution was then stirred for 6 hours at room temperature in the presence of 10% Pd/C (340 mg, 0.32 mmol) under hydrogen gas atmosphere. Insolubles were removed by filtration, and the solvent was distilled off under reduced pressure, to give 779 mg (yield 97%) of the desired compound in the form of a brown crystalline product.

المصدر