تفاعل #9346

معادلة التفاعل

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

المذيبات

Triflic Acid

ظروف التفاعل

المعالجة

1. 1
   أخرىThe resulting waxy solid was purified by chromatography on silica gel

الإجراء التجريبي

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

المصدر