تفاعل #93370
ord-7270018c8e304ab09f9bfd27b2196627
معادلة التفاعل
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1درجة الحرارةwas refluxed for 1 hour
- 2درجة الحرارةAfter cooling, to the mixture
- 3استخلاصThe solution was extracted with chloroform
- 4غسيلThe extract was washed with water
- 5أخرىdried
- 6أخرىevaporated
الإجراء التجريبي
A mixture of 0.39 g of alpha-isopropyl-alpha-[2-[N-[3-(2-methoxyphenoxy)propyl]amino]ethyl]-3,4,5-trimethoxyphenylacetonitrile, 1 ml of 37% formalin, and 1 ml of 90% formic acid was refluxed for 1 hour. After cooling, to the mixture were added water and potassium carbonate to make it alkaline. The solution was extracted with chloroform. The extract was washed with water, dried, and evaporated to give 0.23 g of desired compound as a yellow oil.