تفاعل #9230
ord-e3c1889fcfaf4fb982b73eceaea5d2bc
معادلة التفاعل
1-(6-bromo-2-benzothiazolyl)-3-ethylurea
dppp
triethylamine
styrene
→
desired compound
المردود 62.0%
1-(6-(2(E)-Phenylvinyl)-2-benzothiazolyl)-3-ethylurea
المردود 62.0%
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىwas reacted
الإجراء التجريبي
A mixture of 1-(6-bromo-2-benzothiazolyl)-3-ethylurea, Pd(PPh3)2Cl2, dppp, triethylamine, styrene, and two crystals of BHT in anhydrous DMF was reacted according to the procedure of Example 225 to give the desired compound 0.201 g (62%). LC/MS 324.2 (M+1); LC retention time 2.87 min.