تفاعل #91302
ord-ccde40df819d4a679b4244e8c2673f05
معادلة التفاعل
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
درجة الحرارة
90°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1workup.DISSOLUTIONdissolved in 120 l
- 2درجة الحرارةIt is subsequently cooled to 20° C.
- 3غسيلthe carbon is first washed thoroughly with water)
- 4workup.ADDITIONis added
- 5workup.STIRRINGIt is stirred for one hour at 20° C.
- 6ترشيحthe carbon is subsequently filtered off
- 7غسيلThe carbon is washed three times with 15 l of water each time
الإجراء التجريبي
A total of 3.356 kg calcium carbonate (99.3%) is added in portions to 15.39 kg butrol (water contents: 2.6%) dissolved in 120 l demineralised water and it is stirred for one hour at 90° C. inner temperature. It is subsequently cooled to 20° C. and 1.5 kg active carbon (Norit SX PLUS; the carbon is first washed thoroughly with water) is added. It is stirred for one hour at 20° C. and the carbon is subsequently filtered off. The carbon is washed three times with 15 l of water each time.