تفاعل #91302

ord-ccde40df819d4a679b4244e8c2673f05

معادلة التفاعل

المتفاعلات

الكواشف

لا شيء

المذيبات

ظروف التفاعل

درجة الحرارة
90°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.DISSOLUTIONdissolved in 120 l
  2. 2
    درجة الحرارةIt is subsequently cooled to 20° C.
  3. 3
    غسيلthe carbon is first washed thoroughly with water)
  4. 4
    workup.ADDITIONis added
  5. 5
    workup.STIRRINGIt is stirred for one hour at 20° C.
  6. 6
    ترشيحthe carbon is subsequently filtered off
  7. 7
    غسيلThe carbon is washed three times with 15 l of water each time

الإجراء التجريبي

A total of 3.356 kg calcium carbonate (99.3%) is added in portions to 15.39 kg butrol (water contents: 2.6%) dissolved in 120 l demineralised water and it is stirred for one hour at 90° C. inner temperature. It is subsequently cooled to 20° C. and 1.5 kg active carbon (Norit SX PLUS; the carbon is first washed thoroughly with water) is added. It is stirred for one hour at 20° C. and the carbon is subsequently filtered off. The carbon is washed three times with 15 l of water each time.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US09447053B2uspto-grants-2016_09