تفاعل #91042

ord-8181d3479b6a417fa4adc534e9103e2d

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

2-Chloro-1-ethoxy-5-iodo-3-(pentan-3-yloxy)benzene (8) (1.2 g, 79%) was prepared from 2-chloro-3-ethoxy-5-iodophenol (7) (1.1 g, 3.7 mmol) using a procedure essentially the same as in step (i) for AAA-001 except that 3-bromopentane was used instead of cyclopentyl bromide.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US09447028B2uspto-grants-2016_09