تفاعل #88239

معادلة التفاعل

(3,4-dichlorophenyl)methanamine

4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide

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title compound

4-((3,4-dichlorobenzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide

ظروف التفاعل

المعالجة

1. 1
   أخرىCompound 2 was prepared

الإجراء التجريبي

Compound 2 was prepared following general synthetic scheme 7 wherein (3,4-dichlorophenyl)methanamine was reacted with 4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide to give the title compound. LC-MS [350 (M+1)], 1H NMR (400 MHz, DMSO-d6): δ 9.37 (s, 1H), 9.31 (t, 1H), 8.54 (d, 1H), 8.49 (d, 1H), 8.05 (s, 1H), 8.00 (t, 1H), 7.70 (s, 1H), 7.60 (d, 1H), 7.40 (d, 1H), 4.90 (d, 1H).

المصدر