تفاعل #88131

ord-74d0ce3b928a4390bcc45a40b8c6d8d2

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The title compound, green solid (53 mg, 41%), MS (ISP) m/z=390.2 [(M+H)+], mp 161° C., was prepared in accordance with the general method of example 1 from 1-(2-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate L) (100 mg, 353 μmol) and commercially available 2-(4-fluoro-phenyl)-acetonitrile.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US09440962B2uspto-grants-2016_09