تفاعل #88103

ord-50f4e03be1fd47fea3f8855c699d71d5

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The title compound, light grey solid (74 mg, 56%), MS (ISP) m/z=374.1 [(M+H)+], mp 175° C., was prepared in accordance with the general method of example 1 from 1-(3-fluoro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate D) (100 mg, 353 μmol) and commercially available 2-(4-fluoro-phenyl)-acetonitrile.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US09440962B2uspto-grants-2016_09