تفاعل #88102

ord-fae072bb986f4a439b018eafb7105ddd

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The title compound, light yellow solid (41 mg, 31%), MS (ISP) m/z=374.1 [(M+H)+], mp 159° C., was prepared in accordance with the general method of example 1 from 1-(4-fluoro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate C) (100 mg, 353 μmol) and commercially available 2-(4-fluoro-phenyl)-acetonitrile.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US09440962B2uspto-grants-2016_09