تفاعل #87649

معادلة التفاعل

5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzamide

oxalyl chloride

→

desired product

5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzoyl isocyanate

المذيبات

EDC

ظروف التفاعل

المعالجة

1. 1
   أخرىThe title compound was prepared

الإجراء التجريبي

The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 5-((2,2,2-trifluoroacetamido)methyl)-2-chloro-4-methoxybenzamide (1.0 g, 3.6 mmol), oxalyl chloride (1.0 mL) and EDC (10 mL) to afford 0.750 g of the desired product.

المصدر