تفاعل #86316

معادلة التفاعل

5-bromo-6-methylpyridin-2-amine

N-ethyl-N-isopropylpropan-2-amine

methanesulfonyl chloride

→

title compound

N-(5-bromo-6-methylpyridin-2-yl)methanesulfonamide

المذيبات

DCM

ظروف التفاعل

المعالجة

1. 1
   تركيزwas subsequently concentrated in vacuo

الإجراء التجريبي

To a mixture of 5-bromo-6-methylpyridin-2-amine (0.3 g, 1.604 mmol) and N-ethyl-N-isopropylpropan-2-amine (0.559 mL, 3.21 mmol) in DCM (10 mL) was added methanesulfonyl chloride (0.137 mL, 1.764 mmol) at 0° C. The reaction mixture was stirred at room temperature for 48 hours and was subsequently concentrated in vacuo to give the title compound.

المصدر