تفاعل #848

معادلة التفاعل

p-hydroxybenzoic acid

decanoic acid chloride

pyridine

→

p-decanoyloxybenzoic acid

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   استخلاصan organic layer was extracted with dichloromethane
2. 2
   غسيلThe organic layer was washed with 1N hydrochloric acid
3. 3
   تجفيفdried over anhydrous sodium sulfate
4. 4
   workup.DISTILLATIONthe solvent was distilled off
5. 5
   غسيلresidue was washed with n-hexane
6. 6
   أخرىdried
7. 7
   أخرىto give a crude end product

الإجراء التجريبي

10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.

المصدر