تفاعل #84525

معادلة التفاعل

3-(3-fluorophenyl)propanoic acid

dichlorosulfane

→

title compound

3-(3-fluorophenyl)propanoyl chloride

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةwas refluxed for 3 h
2. 2
   تركيزconcentrated in vacuo

الإجراء التجريبي

A mixture of 3-(3-fluorophenyl)propanoic acid (2.50 g, 14.9 mmol) and dichlorosulfane (10 mL) under N2 was refluxed for 3 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound, which was used for next step without further purification.

المصدر