تفاعل #84025
ord-d872591027264a99a4c357f08f23f73a
معادلة التفاعل
Oxalyl chloride
t-butyl alcohol
→
Compound 34
Chloro-Oxo-Acetic Acid t-Butyl Ester
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThe solvent was evaporated under vacuum
الإجراء التجريبي
Oxalyl chloride (232 μL, 2.8 mmol) and t-butyl alcohol (228 μL) were combined in ether (6.7 mL) under nitrogen at 0° C. The resulting mixture was stirred for 30 minutes at room temperature. The solvent was evaporated under vacuum to form Compound 34.