تفاعل #83783

معادلة التفاعل

2-amino-5-chloropyridine

nitric acid

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title compound

2-Amino5-chloro-3-nitropyridine

المذيبات

sulfuric acid

ظروف التفاعل

المعالجة

1. 1
   أخرىA procedure similar to that described in Preparation 56

الإجراء التجريبي

A procedure similar to that described in Preparation 56 was repeated, except that 25.0 g of 2-amino-5-chloropyridine, 100 ml of concentrated sulfuric acid and 12.5 ml of concentrated nitric acid were used, to give 18.5 g of the title compound, melting at 138°-139° C.

المصدر