تفاعل #833510

معادلة التفاعل

Vanillin

allyl bromide

potassium carbonate

→

3-methoxy-4-(2-propenyloxy)benzaldehyde

المذيبات

acetone

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةAfter cooling
2. 2
   ترشيحthe solid was filtered off
3. 3
   غسيلwashed with acetone
4. 4
   أخرىA yellow oil was obtained
5. 5
   تركيزafter a thorough concentration of the organic phases

الإجراء التجريبي

Vanillin (20.0 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.

المصدر