تفاعل #83345

معادلة التفاعل

2-(4-aminophenylthio)-6-methoxyquinoline

4-chloro-3-trifluoromethylphenylisothiocyanate

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title compound

المردود 72.0%

1-[4-(6-Methoxy-2-quinolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea

المردود 72.0%

ظروف التفاعل

الإجراء التجريبي

2-(4-aminophenylthio)-6-methoxyquinoline (15.0 moles, 4.2 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (15.0 mmoles, 3.6 g) were reacted according to procedure C to yield 5.6 g, 72% of the title compound. Mass Spec (FD) 519. Calculated for C24H17ClF3N3OS2 : C, 55.44; H, 3.30; N, 8.08. Found: C, 55.62; H, 3.43; N, 8.27.

المصدر