تفاعل #82900
ord-3b4cb803a7ea41f7865db932c7cfa3d1
معادلة التفاعل
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1تجفيفthe product is dried in a desiccator over phosphorus pentoxide/potassium hydroxide for 24 h
الإجراء التجريبي
The product from Example 18 is dissolved in trifluoroacetic acid (170 ml) and left at room temperature for 1 h 45 min. Subsequently, the mixture is codistilled five times with toluene and the product is dried in a desiccator over phosphorus pentoxide/potassium hydroxide for 24 h. Yield: 11.8 g (93%).