تفاعل #828717

ord-124348c9e3c74a01bcdfa140f15247e0

معادلة التفاعل

CCOC(C)=O
ethyl acetate
N[C@@H](CCc1ccccc1)C(=O)O
L-HPA
N[C@H](CCc1ccccc1)C(=O)O
D-homophenylalanine

المتفاعلات

الكواشف

لا شيء

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىAfter the completion of the reaction
  2. 2
    أخرىAfter separating the lower layer from the upper layer
  3. 3
    أخرىto obtain D-HPAE, which

الإجراء التجريبي

After the completion of the reaction, an extractant such as ethyl acetate is added to the reaction mixture which separates the reaction mixture into an upper layer and a lower layer. The upper layer contains D-HPAE in the organic solvent and the lower layer contains L-HPA in water. After separating the lower layer from the upper layer, the extractant, i.e., ethyl acetate, can be vaporized to obtain D-HPAE, which can be chemically hydrolyzed to obtain D-homophenylalanine.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05552317uspto-grants-1996_09