تفاعل #828712
ord-9595334a782f420e929bf7c210e29da7
معادلة التفاعل
9-borabicyclo[3.3.1]nonane
HCl
→
title compound
المردود 75.0%
B-chloro-9-borabicyclo[3.3.1]nonane
المردود 75.0%
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The title compound was prepared in 75% yield following the method of Example 1 by treating 9-borabicyclo[3.3.1]nonane (9-BBN, Aldrich Chemical Company, Inc., Milwaukee, Wis.) with anhydrous HCl in ether. 11B NMR δ 79 ppm in hexane, bp 65° C. (0.3 mm).