تفاعل #8286

معادلة التفاعل

4-acetoxy-3-phenyl-but-2-enoic acid methyl ester

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title compound

المردود 92.2%

4-Acetoxy-3-phenyl-butyric acid methyl ester

المردود 92.2%

المذيبات

acetic acid

ظروف التفاعل

المعالجة

1. 1
   ترشيحThe mixture is filtered through a pad of Celite®
2. 2
   غسيلrinsed with methanol
3. 3
   تركيزThe solution is concentrated in vacuo

الإجراء التجريبي

A mixture of 4-acetoxy-3-phenyl-but-2-enoic acid methyl ester, (1.0 g, 4.27 mmol), 10 wt. % palladium on activated carbon (1.0 g), acetic acid (10 mL) is shaken under an atmosphere of hydrogen on a Parr® Shaker. The mixture is filtered through a pad of Celite® and rinsed with methanol. The solution is concentrated in vacuo to yield 0.93 g (92%) of the title compound.

المصدر