تفاعل #822566

ord-bdf0c8acb3d9432eb47da929020ce2cc

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىa yellow solid is obtained (0.77 g; yield=63%; m.p.=145° C.)

الإجراء التجريبي

In a manner similar to that of Example 7d, by reacting 1.28 g (2.5 mmol) of methyl 4-(8,8-dimethyl-5-p-tolyl-7,8-dihydro-2-naphthylselanylethynyl)-2-fluorobenzoate with 0.51 g (13 mmol) of sodium hydroxide, a yellow solid is obtained (0.77 g; yield=63%; m.p.=145° C.).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07592478B2uspto-grants-2009_09