تفاعل #821344

ord-9cc4c8921e6e4e4da953694505dfc186

معادلة التفاعل

OC[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O)CO
Diglycerol
OC[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O)CO
(1) Sorbitol
O=C1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O
Gluconolactone
OC[C@H]1O[C@@](CO)(O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@@H](O)[C@@H]1O
Sucrose
→
C=C(C)C(=O)O.C=Cc1ccccc1C=C
Divinylbenzene Methacrylic Acid

المتفاعلات

—
( 1 )
—
( 6 )
OC[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O)CO
Diglycerol
OC[C@@H](O)[C@H](O)[C@@H](O)[C@@H](O)CO
(1) Sorbitol
—
Divinylbenzene methacrylic acid copolymer 1
O=C1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O
Gluconolactone
—
( 4 )
—
Zeolite
OC[C@H]1O[C@@](CO)(O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@@H](O)[C@@H]1O
Sucrose
—
( 2 )
—
( 5 )

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    درجة الحرارةheat at 90 to 120 C
  2. 2
    workup.ADDITIONmix
  3. 3
    أخرىAn opaque mobile sticky liquid is obtained

الإجراء التجريبي

Ingredients. (1) Diglycerol 10.0 (2) Sucrose 74.0 (3) Gluconolactone (10% solution in water) 10.0 (4) Preservative 1.0 (5) Divinylbenzene/methacrylic acid copolymer 1.0 (6) Zeolite 4.0. Procedure. Mix (2) to (5) and heat at 90 to 120 C. for 30 to 45 minutes to a clear liquid. Add (1) and (6) and mix. Cool to room temperature. An opaque mobile sticky liquid is obtained.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07592002B2uspto-grants-2009_09