تفاعل #821334

ord-02cd26076f4944fcb1da7dcd39b0dc3f

معادلة التفاعل

Cl.Cl.Nc1c(F)c(N)c(F)c(F)c1F
dihydrochloride
Cc1cc(NC(CO)CO)ccc1[N+](=O)[O-]
2-(4-nitro-3-methylphenylamino)propane-1,3-diol
Cc1cc(NC(CO)CO)ccc1N.Cl.Cl
amine
Cc1cc(NC(CO)CO)ccc1N.Cl.Cl
2-(4-amino-3-methylphenylamino)propane-1,3-diol Dihydrochloride

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The 2-(4-nitro-3-methylphenylamino)propane-1,3-diol (11) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07591860B2uspto-grants-2009_09