تفاعل #81687

ord-6a4a9d71f6204543b7bc12d011dc8c18

معادلة التفاعل

c1ccc(Nc2ccccc2)cc1
diphenylamine
O=C1CCCCC1
cyclohexanone
Nc1ccccc1
aniline
c1ccc(N(c2ccccc2)c2ccccc2)cc1
triphenylamine
O=[N+]([O-])c1ccccc1
nitrobenzene
c1ccc(NC2CCCCC2)cc1
N-cyclohexylaniline
المردود 2.9%

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىReaction

الإجراء التجريبي

Reaction was carried out by the same procedure as in Example I1 except that 32.39 g (0.39 mol) of cyclohexanone, 9.31 g (0.1 mol) of aniline and 24.62 g (0.2 mol) nitrobenzene were used. As a result, the yield of diphenylamine was 89.5%, and 1.8% of triphenylamine and 2.9% of N-cyclohexylaniline were produced.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05618980uspto-grants-1997_04