تفاعل #8164

ord-c9ce789e8e2a4048869aacc55103453f

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Similar to Example 1, equimolar amounts of 3-chlorophenylhydrazine hydrochloride and 2-acetyl-3-oxo-butyric acid ethyl ester were combined in a solution of 50% pyridine in ethanol. Analysis confirmed that the resulting solid was determined to be the named product (m.p. 56° C.–57° C.).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07087634B2uspto-grants-2006_08