تفاعل #816375

ord-025a511458114e689c858c6d71844f4b

معادلة التفاعل

Cc1c(N)c(=O)n(-c2ccccc2)n1C
4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
Cc1cccc(O)c1
meta-cresol
N
ammonia
CC1=CC(=O)C=C/C1=N/c1c(C)n(C)n(-c2ccccc2)c1=O
1,5-dimethyl-4-{[(1Z)-2-methyl-4-oxocyclohexa-2,5-dien-1-ylidene]amino}-2-phenyl-1,2-dihydro-3H-pyrazol-3-one

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىranging from 5 to 10° C.

الإجراء التجريبي

10 mmol of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in 30 ml of water. This solution was admixed with 10 mmol of meta-cresol in solution in 30 ml of 2-propanol, 3 ml of 20% aqueous ammonia and 22 mmol of potassium ferricyanide at a temperature ranging from 5 to 10° C.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07582123B2uspto-grants-2009_09