تفاعل #816375
ord-025a511458114e689c858c6d71844f4b
معادلة التفاعل
4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
meta-cresol
ammonia
→
1,5-dimethyl-4-{[(1Z)-2-methyl-4-oxocyclohexa-2,5-dien-1-ylidene]amino}-2-phenyl-1,2-dihydro-3H-pyrazol-3-one
الكواشف
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىranging from 5 to 10° C.
الإجراء التجريبي
10 mmol of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in 30 ml of water. This solution was admixed with 10 mmol of meta-cresol in solution in 30 ml of 2-propanol, 3 ml of 20% aqueous ammonia and 22 mmol of potassium ferricyanide at a temperature ranging from 5 to 10° C.