تفاعل #806241

ord-eef5c588dd4c4f47bac0fab60972a05c

معادلة التفاعل

O
water
Oc1ccccc1
Phenol
Oc1ccccc1
Phenol
Oc1ccccc1
Phenol
Oc1ccccc1
Phenol
Oc1ccccc1
Phenol
Oc1ccccc1
Phenol
Oc1ccccc1
Phenol
O=S(=O)(O)O
sulfuric acid
O=S(=O)(O)c1ccc(O)cc1
Phenolsulfonic acid

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىwas at a temperature of 95 degrees Centigrade

الإجراء التجريبي

Phenolsulfonic acid solution was prepared in sulfuric acid. The method included setting up a recirculating water bath so that the water was at a temperature of 95 degrees Centigrade. Next, the weight of available stock of Liquified Phenol USP containing 3.23 moles of Phenol was calculated. Phenol has a molecular weight of 94.11. The weight of 3.23 moles of Phenol is 3.23×94.11+303.97 grams. The purity of Liquified Phenol USP typically ranges from 89.0% to 91.5%. Using the purity value either from the manufacturer's Certificate of Analysis or the purity value from an internal quality control analysis, the weight of the available stock of Liquified Phenol USP required to deliver 3.23 moles of Phenol was calculated.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07132111B2uspto-grants-2006_11