تفاعل #80567

ord-8e4b4b7fd8854a2684e0c0c78407b175

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    workup.ADDITIONis then added with magnetic stirring
  2. 2
    درجة الحرارةThe reaction mixture is cooled in an ice bath

الإجراء التجريبي

0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05616614uspto-grants-1997_04